(sh)ӛ¼(yng)(dng)Crԭʼ挍(sh)Ҏ(gu)wҊƄ(sh)ӛ¼Ҏ(gu)(sh)ӛ¼(yng)(dng)EױJ(rn)
(sh)ӛ¼üy(tng)һʹÌ(sh)ӛ¼ʹ֪Ŀ¼IJֽM
һ(sh)ӛ¼ֻӛ¼һоĿSӛ¼cҎ(gu)ĿoP(gun)ă(ni)ݡ
(sh)ӛ¼ġĿQĿ̖Լӛ¼̖@ӛ¼ˆTP(gun)Ϣӛڃ
S(sh)M(jn)չ(sh)ˆT(yng)(dng)ra(b)䌍(sh)?zi)?frac14;Ŀ¼(sh)QP(gun)퓴a
(sh)ӛ¼һr(yng)(dng)QÙM(bio)עֻúɫ{(ln)ɫ䓹Pɫ{(ln)ɫֹPұCӛ¼wֹPEɫy(tng)һ
õӢĿs(sh)ԇĿs(yng)(dng)Ҏ(gu)ڳõJ(rn)״γF(xin)rļע(sh)ӛ¼Ќgĵ(yng)(dng)עīI(xin)QԴϢ
(sh)ӛ¼(yng)ʹҎ(gu)ČI(y)g(sh)ZӋλ(yng)ÇH(bio)(zhn)ӋλͨӋλЧ(sh)ֵȡᑪ(yng)M㌍(sh)Ҫ
(sh)ӛ¼Sģ̎һбͿCǰӛ¼܉J(rn)P(gun)Ҫ(sh)(j)ҪP(gun)ˆTעĕrgԭrP(gun)ؓ(f)؟(z)ˏ(f)˲֡
xõČ(sh)DDVƬȑ(yng)ճNڌ(sh)ӛ¼(yng)λTpִ_J(rn)YҪ(bio)(sh)(ni)ȺbӆɃ
һ퓌(sh)ӛ¼ֻӛ¼ͬһĹSӛ¼ĹP(gun)(sh)Y(ji)ӛ¼߀ʣհ횏Ŀհ̎Ϸ·һббɂ(c)ɢό(sh)˵
ÿһӛ¼Ŀ̖ӛ¼̖߀עϽ퓴a½퓴a
ӛ¼IJְ(ni)ݣ(sh)Q(sh)?zi)?sh)ԭϼO(sh)(sh)^̡Y(ji)c(sh)Y(ji)Փ
(sh)Q
ÿһ(sh)(yng)(dng)һҪQ̫Ҳ^L
磺
漰ķ(yng)ȴNcķ(yng)˿캬ˮ(yng)Ӱ(sh)Q顰ij(yng)ˮֵӰ푡
(sh)?zi)ģ?/span>
Ҫf(sh)O(sh)ӋĿģԼҪ_(d)Ч
磺
Ȼ(sh)(sh)?zi)Ŀ顰ˮֺڷ?yng)Ӱ푡
(sh)ԭ
O(sh)Ӌԓ(sh)ĻԭԼW(xu)(yng)ʽDžīI(xin)Ҏ(gu)YO(sh)ӋČ(sh)߀Ԕ(x)(bio)עÁԴ
磺
1(yng)ʽ
2(yng)܄ijijм벻ͬˮԺ(yng)׃
3(sh)
1 |
2 |
3 |
4 |
|
ȴN |
5mL5.75g |
|||
|
20mL13.8g~4eq |
|||
ˮ |
2%V0.4mL |
4%V0.8mL |
6%V1.2mL |
8%V1.6mL |
ض |
Ҝ |
|||
(yng)rg |
6h |
|||
|
cˮϣַşԺȴN](yng)wϵ6h |
ϼO(sh)䣺
Ԕ(x)ʹϵQԭϼeȣ̖a(chn)S̵ȻϢʹõăxO(sh)Ҫע̖
磺
Q |
|
e |
̖ |
S |
ȴN |
98% |
I(y) |
LTM20160503 |
*****S |
|
95% |
I(y) |
ATM20160628 |
*****˾ |
(sh)^̣
(yng)(dng)Ԕ(x)ӛ¼^̡^쵽ĬF(xin)Ӱص(sh)^nj(sh)ӛ¼ĺă(ni)ݣҪԔ(x)挍(sh)
磺
1 |
2 |
3 |
4 |
|
8:40 |
ȡĂ50mLAןƿ20mL |
|||
8:50 |
ˮ |
|||
0.4mL |
0.8mL |
1.2mL |
1.6mL |
|
ˮԺwϵضȾˮԽĜضҕԽ^m(x)ʹş |
||||
9:05 |
ĂƿӸ5mLȣ^m(x)ؔ |
|||
9:10 |
F(xin)ɫw |
|||
9:20 |
F(xin)ɫw |
|||
9:30 |
F(xin)ɫw |
|||
9:45 |
F(xin)ɫw |
|||
15:10 |
(yng)ѽ(jng)6h |
15:35 |
pضȞ45ĿDZMɶİ |
16:05 |
Y(ji)l(f)F(xin)wϵόһ͠|(zh) |
17:00 |
Y(ji)Qصõ94.00ga(chn)Ʒ؞94.00 - 65.00 = 29.00g ȡ͙zHPLC̖SHTM-170825-5 |
17:10 |
a(chn)Ʒڱб棨̖XXX |
Y(ji)c
(zhn)_ӛ¼^ָ(bio)Ĕ(sh)(j)׃ÿ헌(sh)Y(ji)(yng)M(jn)Д(sh)(j)̎ͷСY(ji)
磺
HPLCewһ
3.2min |
7.8mina(chn) |
12.5minԭ |
20.3min |
|
SHTM-170825-1 |
0.3 |
94 |
0.5 |
2.0 |
SHTM-170825-2 |
0.4 |
97 |
0.1 |
1.5 |
SHTM-170825-3 |
0.4 |
98 |
0 |
1.2 |
SHTM-170825-4 |
0.5 |
94 |
0 |
3.8 |
SHTM-170825-5 |
0.4 |
96 |
0.1 |
2.2 |
3M4M(yng)a(chn)a(chn)4M(yng)20.3mins|(zh)
(sh)Y(ji)Փ
(j)(sh)Y(ji)ó(sh)Y(ji)Փ
磺
(sh)Cˮ4%~6%(yng)s|(zh)^a(chn)HPLCeֺ
c(f)ˣ
(dng)Ռ(sh)Y(ji)(sh)ӛ¼·Ҏ(gu)հ̎Ŀؓ(f)؟(z)ˌ˺вҪڙz錍(sh)ӛ¼zҊ
(sh)ӛ¼(yng)(dng)Ʊˮī߅SκͿĨa(b)ȱ퓡հО
I(lng)
(sh)ˆT(sh)ӛ¼I(lng)ȡՈΡ(jng)в(zhn)ԺвˆT̎I(lng)ӛI(lng)ȡӛ¼ǰ(yng)J(rn)xļԼӛ¼еġʹ֪Ҏ(gu)λ̎ʹ{(ln)ɫɫP
wn
r회(sh)ӛ¼wn(sh)ӛ¼ʹꮅĿY(ji)(sh)ˆTx(sh)ˆT{(dio)
wnrĿ¼ĿհҪϷ·һббɂ(c)քeڣIJֵĿհҲҪϷ·һббɂ(c)ڣ(bio)עԺհס
(sh)ӛ¼P(gun)Twnӛ¼ˆT회wnϢĿ¼֏(f)ӡ_~ӆɃ
ӛ¼ˆT회Ϣrӛ
£֣ԴW(wng)j(lu)С
ѣDƬЃ(ni)HڌW(xu)(x)֙(qun)(ni)ݼ淨(ni)Ոr(lin)ϵhش